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In situ synchrotron radiation monitoring of phase transitions during microwave heating of Al-Cu-Fe alloys

Vaucher, Sébastien ; Nicula, Radu ; Català-Civera, José-Manuel ; Schmitt, Bernd ; Patterson, Bruce

In: Journal of Materials Research, 2008, vol. 23, no. 1, p. 170-175

A von Hamos x-ray spectrometer based on a segmented-type diffraction crystal for single-shot x-ray emission spectroscopy and time-resolved resonant inelastic x-ray scattering studies

Szlachetko, Jakub ; Nachtegaal, M. ; Boni, E. de ; Willimann, M. ; Safonova, O. ; Sa, J. ; Smolentsev, G. ; Szlachetko, Monika ; Bokhoven, J. A. van ; Dousse, Jean-Claude ; Hoszowska, Joanna ; Kayser, Yves ; Jagodziński, P. ; Bergamaschi, A. ; Schmitt, Bernd ; David, Christian ; Lücke, A.

In: Review of Scientific Instruments, 2012, vol. 83, no. 10, p. 103105

We report on the design and performance of a wavelength-dispersive type spectrometer based on the von Hamos geometry. The spectrometer is equipped with a segmented-type crystal for x-ray diffraction and provides an energy resolution in the order of 0.25 eV and 1 eV over an energy range of 8000 eV–9600 eV. The use of a segmented crystal results in a simple and straightforward crystal...

Amino acids in iron oxide mineralization: (incomplete) crystal phase selection is achieved even with single amino acids

Mantion, Alexandre ; Gozzo, Fabia ; Schmitt, Bernd ; Stern, Willem B. ; Gerber, Yvonne ; Robin, Adeline Y. ; Fromm, Katharina M. ; Painsi, Monika ; Taubert, Andreas

In: The Journal of Physical Chemistry C, 2008, vol. 112, no. 32, p. 12104–12110

Iron oxides are important minerals in biology and materials science. Using biomimetic synthesis, a variety of iron oxides have been fabricated. However, it is still not clear how growth modifiers like amino acids and peptides select different crystal phases of a complex material like iron oxide. The current paper shows that already with single amino acids, (incomplete) crystal phase selection is...